有机化学实验

出版时间：2011-11  出版社：高等教育出版社  作者：王梅，等 编  页数：234  

内容概要

　　This book is compiled on the basis of "Organic Chemistry Experiments" （fourth edition， edited by Zhanxian Gao） and with combination ofthe bilingual teaching experience.　　The book encompasses six sections： introduction， basic techniques for organic experiments， basic preparation experiments of organic compounds，comprehensive experiments， self-designing experiments， and investigative experiments. Tables of commonly used data， index， and the Chinese-English professional glossary are attached to the end ofthe book.　　The book was written with emphasis on （1） basic techniques for organic experiments， including some advanced experimental techniques such as microwave reactions and the resolution of racemates; （2） common scale and miniscale experiments， also taking account of semimicro- and microscale experiments;（3） traditional and representative organic reactions， meanwhile，　　introducing the concept of "green" synthesis; and （4） training students in basic experimental skills， including developing their ability in experimental design and scientific research as well.　　This book can be used as a textbook for the bilingual course of organic chemistry experiments. It can also be used as a teaching reference book for the experiment courses of other related majors.

书籍目录

Chapter 1 Introduction1.1 General Rules for Organic Chemistry Laboratory　1.2 Safe Laboratory Practice and First Aid in Case of an Accident 1.2.1 Prevention of Fires and First Aid in Case of a Fire　1.2.3 First Aid for Cuts and Scalds　1.2.4 Prevention of Damages from Hazardous Chemicals and First Aid for Chemical Burns1.2.5 Toxicity and Safety Data of Chemicals 1.2.6 Disposal of Chemical Wastes　1.3 Informatiori Sources for Experimental Organic Chemistry1.3.1 Important Handbooks and Dictionaries1.3.2 Important Journals Involving Organic Experiment 1.3.3 Important Online Resources　1.4 Common Glassware and Apparatus1.4.1 Names and Uses of Common Glassware 1.4.2 Cleaning and Drying Glassware1.4.3 Common Organic Lab Apparatus1.4.4 Assembling and Disassembling Apparatus　1.5 Preparation and Notebook for the Laboratory 1.5.1 Laboratory Preparation Note1.5.2 Experimental Record1.5.3 Sample Calculation for Notebook Records1.5.4 Laboratory Notebook Formats1.5.5 Experimental ReportChapter 2　Basic Techniques for Organic Experiments2.1 Working on Glass Tubes2.1.1 Cutting and Bending Glass Tubes　2.1.2 Stretching Glass Tubes 2.2　 Weighing, Measuring and Transferring Reagents2.2.1 Measuring and Transferring Liquids2.2.2 Weighing Methods2.3　Heating, Cooling and Stirring Methods2.3.1 Heating Methods and Precautions2.3.2 Cooling Methods and Coolants2.3.3 Stirring Methods and Equipment2.4 Extraction2.4.1 Liquid-Liquid Extraction2.4.2 Liquid-Solid Extraction2.5 Drying and Drying Agents2.5.1 Drying Organic Liquids2.5.2 Drying Solids2.6 Gas Traps2.7 Separating and Purifying Liquid Compounds2.7.1 Simple Ddstillation2.7.2 Fractional Distillation2.7.3 Vacuum Distillation2,7.4 Steam Distillation 2.8 Separating and Purifying Solid Compounds2.8.1 Filtration Apparatus and Techniques 2.8.2 Centrifugation and Decanting Solutions2.8.3 Evaporatine Solvents2.8.4 Decolorizing Carbon2.8.5 Recrystallization2.8.6 Sublimation 2.9 Chromatography2.9.1 Column Chromatography　2.9.2 Thin-Layer Chromatography （TLC）2.9.3 Gas Chromatography （GC）2.9.4 High-Performance Liquid Chromatography （ HPLC）2.10 Measuring Physical Constants of Organic Compounds2.10.1 Melting Point 2.10.2 Boiling Point2.10.3 Refractive Index 2.10.4 0ptical Rotation and Specific Rotation 2.10.5 Relative Density2.11 Spectroscopic Identification of Organic Compounds2.11.1 Infrared （IR） Spectroscopy 2.11.2 Nuclear Magnetic Resonance （NMR） Spectroscopy2.11.3 Ultra-Violet-Visible （UV-Vis） Spectroscopy……Chapter 3 Basic ExperimentsChapter 4 Comprehensive ExpermentsChapter 5 Self-Designing ExperimentsChapter 6 Investigative ExperimentsReferencesAppendixIndexVocabularyPeriodic Table of the Elements